3D Bioplotter Research Papers
Displaying all papers by M. Laugesen (1 results)
Precision lattice parameter determination from transmission diffraction of thick specimens with irregular cross sections
Journal of Applield Crystallography
2019
Volume 52, Pages 40-46
Accurate determination of lattice parameters from X-ray diffraction requires that the diffraction angles be measured very precisely, and significant errors result if the sample–detector separation differs from that assumed. Transmission diffraction from bones, which have a complex cross section and must be left intact, is a situation where this separation is difficult to measure and it may differ from position to position across the specimen. This article describes a method for eliminating the effect of variable sample cross section. Diffraction patterns for each position on the specimen are collected before and after 180° rotation about an axis normal to the…